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Synthesis, Properties, and Two-Dimensional Adsorption Characteristics of [6]Hexahelicene-7-carboxylic acid.

Maarten W van der Meijden,Tatyana Balandina,Oleksandr Ivasenko,Steven De Feyter,Klaus Wurst,Richard M Kellogg

CHEMISTRY-A EUROPEAN JOURNAL（2016）

Cited 8|Views18
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Abstract
A convergent synthesis of racemic [6]hexahelicene-7-carboxylic acid by cross-coupling of a bicyclic and a tricyclic component is described. A metal-catalyzed ring-closure is also a fundamental component of the synthetic approach. Scanning tunneling microscopy (STM) measurements of the racemate self-assembled on Au(111) at liquid-solid interface revealed the formation of ordered racemic 2D crystals.
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Key words
acid functionalization,cross-coupling,helicene,metal catalyzed cyclizations,scanning tunneling microscopy
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