Effect of Process Atmosphere on Microstructure, Melt Pool, Texture, Precipitate Characteristics, and Mechanical Properties of Laser Powder Bed Fusion Fe-12Cr-6Al

Omer Cakmak,Seong Gyu Chung, Seung-Hoon Lee, JiHoe Koo,Hwasung Yeom,Jung-Wook Cho

Additive Manufacturing Letters(2024)

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Abstract
This study investigates the impact of atmospheres (Ar and N2) on Fe-12Cr-6Al alloy fabricated using laser powder bed fusion (L-PBF) in terms of melt pool shape/size, microstructure, precipitate characteristics, and mechanical properties. The sample built in the N2 atmosphere exhibited lower porosity, wider melt pools, and no Al2O3 agglomeration. Oxygen content decreased from 0.012 to 0.0045 (wt. %), and nitrogen content increased from 0.013 to 0.02 (wt. %). The Ar-printed sample had a yield strength (YS) of 232 ± 15 MPa, ultimate tensile strength (UTS) of 286 ± 10 MPa, and total elongation (TE) of 6.4 ± 1.3%, while the N2-printed sample showed significant improvements of the mechanical properties: YS of 315 ± 11 MPa, UTS of 401 ± 11 MPa, and TE of 7.8 ± 1.1%. Therefore, N2 might be considered to replace Ar as a cost-effective shielding gas for FeCrAl alloys, with improved properties.
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Key words
Process atmosphere effect,In-situ synthesis of precipitates,Microstructure,Mechanical properties,L-PBF,Nitrides,Oxides
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