Highly radiation-stable DLC coatings for a new class of detectors: Structural and morphological features

Within the framework of the FTM-NEXT INFN (Fast Time Micropattern gaseous detectors - next of Nuclear Physics National Institute) experiment, we produced hydrogen -free diamond-like carbon films through pulsed-laser deposition to serve as resistive layers in modern resistive micro -pattern gaseous detectors that must work in extreme radiation environments at future colliders. To obtain homogeneous diamond-like carbon coatings, over medium -to -large size (3 cm x 3 cm), with excellent adhesion to the substrate and with typical surface resistivity values in the range of 1 - 100 MOhm/sq, growth conditions had to be optimized. In this paper we report on the stability of resistive diamond-like carbon layers subjected to increasing doses of irradiation with proton beams accelerated to an energy of 2 MeV. The morphological, structural, and electrical properties, also at the nanoscale level, of diamond-like carbon coatings following ion irradiation were studied by electron microscopy, electron diffraction, electrical transport characterization and scanning tunneling spectroscopy.