Strong textured Sm 2 (CoFeTi) 17 nano-flakes prepared by surfactant-assisted ball milling

Indian Journal of Physics(2024)

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摘要
Sm 2 Co 14.75 Fe 1.5 Ti 0.75 nano-flakes have been prepared by surfactant-assisted ball milling (SABM) in the organic solvent of heptane with the surfactants of oleic acid. The effects of ball milling time on phase composition and magnetic properties were systematically studied. The experimental results show that the synthesized nano-flakes have an amorphous phase and a hexagonal 2:17-type crystalline phase with [00l] in-plane crystallographic texture induced by SABM without any external magnetic field. The coercivity value of the as-prepared nano-flakes was 5.0 kOe and then was enhanced to 6.0 kOe by the magnetic alignment for the sample ball-milled for 4 h. The remanence value of the un-aligned nano-flakes is lower than that of the magnetically aligned ones. In addition, the magnetically aligned nano-flakes exhibit a maximum energy product (BH) max of 56 kJ/m 3 and a small misalignment angle θ of 11°, which is the best value ever reported. The magnetic anisotropy behavior was also observed in both aligned and un-aligned nano-flakes.
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关键词
Nano-flakes,Crystallographic texture,Surfactant-assisted ball milling (SABM),Anisotropy
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