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Effect of Conditions on Anisole Deoxygenation in Supercritical n -Hexane in the Presence of a Palladium Catalyst

A. A. Dmitrieva, S. D. Emelyanova,A. A. Stepacheva,V. G. Matveeva,M. G. Sulman

Russian Journal of Physical Chemistry B（2023）

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Abstract
The effect of the temperature, pressure, and gas phase composition on anisole deoxygenation in supercritical n -hexane in the presence of a palladium catalyst supported on hypercrosslinked polystyrene is studied. The maximum yield of aromatic products (benzene, toluene) is obtained under the following conditions: a temperature of 270°C and an initial pressure of the nitrogen–hydrogen mixture (20 vol % H 2 ) of 1.5 MPa.
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Key words
anisole,deoxygenation,supercritical hexane,aromatic hydrocarbons
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