New Tetraruthenium Cluster from the Thermolysis of [Ru3(CO)10(μ-dppm)]: Crystal Structure of [HRu4(CO)9(μ3-PhPCH2PPh2) (μ3,η2:η1:η1-C6H4)]

Md. Abdullah Al Mamun,Tazul Islam,Subas Rajbangshi,Shishir Ghosh,Michael G. Richmond,Shariff E. Kabir

Journal of Chemical Crystallography（2023）

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摘要

Thermolysis of [Ru3(CO)10(μ-dppm)] (1) in refluxing benzene, followed by chromatographic separation by TLC, afforded the new cluster [HRu4(CO)9(μ3-PhPCH2PPh2)(μ3,η2:η1:η1-C6H4)] (10) in 7

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关键词

Ruthenium carbonyl cluster, Diphosphine activation, P–C and C–H bond scission, X-ray structure, DFT

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