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In situ study of the evolution of NiFe nanocatalysts in reductive and oxidative environments upon thermal treatments

François Robert,Pierre Lecante,Jean‐Sébastien Girardon,Robert Wojcieszak,Éric Marceau,Valérie Briois,Catherine Amiens,Karine Philippot

Faraday Discussions（2023）

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Abstract
XAS monitoring of the reduction of partially oxidized NiFe nanoparticles evidenced an internal redox phenomenon induced by a residual Ni core, before complete reduction occurred with a change in the chemical structure from core–shell to alloy.
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Key words
nife nanocatalysts,oxidative environments
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