Dual grain size-effects on hydrogen-assisted fatigue crack growth in 1 GPa-class medium-carbon martensitic steel

The influence of prior austenite grain (PAG) size ranging from 6 to 90 mm on the fatigue crack growth (FCG) of a tempered 0.41%C lath martensitic steel was investigated in a 90 MPa H2 gas environment at ambient temperature. Under the presence of H, severe FCG accelerations accompanying intergranular (IG) cracking along PAG boundaries as well as quasi-cleavage (QC) fracture along martensite block boundaries and {011} crystallographic planes were systematically found. Smaller PAG mitigated the acceleration at a relatively high-stress intensity via suppressing IG cracking. However, PAG refinement instead escalated the acceleration at a low-stress intensity factor where QC facture prevailed. This inverse grain size effect was discussed in terms of the plasticity criterion in triggering QC and its possible dependence on the microstructural length scale. (c) 2023 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved.