Crystal structure of (8R,8S,13S,13R)-8,8-bis(hydroxymethyl)-9,9,10,10-tetramethoxy-5,5, 6,6,8,8,13,13-octahydro-[13,13-bi[1,3]dioxolo[4,5-g]isoquinolino[3,2 -a]isoquinoline]-7,7-diium chloride-methanol (1/2), C₄₆H₅₈N₂O₁₄Cl₂

ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES（2024）

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摘要

C46H58N2O14Cl2, triclinic, P 1 (no. 2), a = 7.5623(2) & Aring;, b = 10.87056(17) & Aring;, c = 13.90486(15) & Aring;, alpha = 105.7122(12)degrees, beta = 98.907(2)degrees, gamma = 91.067(2)degrees, V = 1084.88(4) & Aring;(3), Z = 1, R-gt(F) = 0.0341, wR(ref)(F-2) = 0.0935, T = 100(2) K.

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Crystal structure of (8R,8S,13S,13R)-8,8-bis(hydroxymethyl)-9,9,10,10-tetramethoxy-5,5, 6,6,8,8,13,13-octahydro-[13,13-bi[1,3]dioxolo[4,5-g]isoquinolino[3,2 -a]isoquinoline]-7,7-diium chloride-methanol (1/2), C46H58N2O14Cl2

Crystal structure of (8R,8S,13S,13R)-8,8-bis(hydroxymethyl)-9,9,10,10-tetramethoxy-5,5, 6,6,8,8,13,13-octahydro-[13,13-bi[1,3]dioxolo[4,5-g]isoquinolino[3,2 -a]isoquinoline]-7,7-diium chloride-methanol (1/2), C₄₆H₅₈N₂O₁₄Cl₂