Mechanical properties evolution of clays treated with rice husk ash subjected to freezing-thawing cycles

Rapidly growing urbanization and industrialization drive the continued development of soil stabilization and ground improvement techniques. Rice husk ash (RHA) is widely regarded as a highly promising construction material in civil engineering due to its excellent pozzolanic properties and has garnered significant attention from researchers. This paper presents an experimental study and a micro-mechanical discussion on the role of RHA in the mechanical improvement of soil. RHA was mixed with the native soil in varying proportions, ranging from 0% to 12%. Several laboratory tests were conducted, including standard proctor compaction tests, Atterberg limit tests, freeze-thaw tests, unconfined compression tests, X-ray diffraction (XRD) analysis, and scanning electron microscopy (SEM). The results indicated that the optimal moisture content (OMC) of the soil mixture increased while the maximum dry density (MDD) decreased with higher RHA dosage. The Atterberg limits of the soil mixture exhibited a positive correlation with the RHA content. A substantial enhancement in the soil's strength, stiffness, and ductility was observed upon the incorporation of RHA. It was noted that the strength loss of the untreated samples and those with 12% RHA was 34.91% and 12.89%, respectively, following 12 freeze-thaw cycles. Furthermore, XRD test results revealed that the treated specimen had an identical mineral composition to the control specimen, with no generation of hydration products. SEM analysis also highlighted that the filling effect of RHA significantly reduced pore content and pore connectivity within the soil, accompanied by a shift in the specimen's pores from mesopores to small and micropores. The excellent thermal insulation and heat retention properties of RHA, along with its pore-refining effect, make a positive contribution to enhancing the frost resistance of the specimens. These findings contribute to guiding the effective application of RHA in civil engineering, offering eco-friendly solutions for biomass waste management, and promoting the sustainable development of construction materials.