Preparation of enriched Boron (11B, 10B) targets using sedimentation method on polymer backing

R. Mondal Saha,K. Banerjee,T. K. Rana,N. Gayathri, G. Pramanik, S. Dey, S. Kundu,S. Manna, P. Pant, R. Shil, P. Roy, T. K. Ghosh,A. Sen,R. Pandey, G. Mukherjee,A. Roy, C. Bhattacharya

NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT(2023)

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摘要
Isotopically enriched boron targets of a typical thickness 1.8 mg/cm(2 )were fabricated on polymer (polypropylene and Mylar) backing using the sedimentation method. Polyvinyl alcohol (PVA) was used as a binder in this target preparation. It was observed that without including an additional PVA layer, boron spills off during ion beam exposure. Adding a PVA layer may produce defects in target, which were identified and discussed. Targets were characterized for thickness uniformity, surface defect and elemental purity using alpha-spectroscopy, optical microscopy, Fourier Transform Infrared spectroscopy (FTIR) and X-ray diffraction (XRD) techniques. Ion beam experiment shows that polypropylene-backed targets are more prone to degrade during beam exposure. No such effect was observed for the target with Mylar backing instead of having a higher thickness than polypropylene.
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关键词
Enriched boron,Nuclear target,Sedimentation,Characterization,XRD,FTIR,Optical microscopy
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