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Polyalkoxy-substituted nitrostilbenes in the synthesis of lamellarin analogs. Formal synthesis of lamellarin H

E. A. Silyanova, A. S. Maksimenko, M. D. Brunner, I. A. Koblov,V. P. Kislyi,A. V. Samet,V. V. Semenov

RUSSIAN CHEMICAL BULLETIN（2023）

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Abstract
Lamellarin D trimethyl ether was prepared by 1,3-dipolar cycloaddition of 6,7-dimethoxyisoquinolinium ylide to pentamethoxy-substituted nitrostilbene followed by a lactone ring closure in the intermediate cycloadduct. This approach allowed a formal synthesis of lamellarin H.
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Key words
essential oils,Acorus calamus,azarone,isoquinolinium ylides,nitrostilbenes,1,3-dipolar cycloaddition,lamellarin D trimethyl ether,lamellarin H,formal synthesis
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