Assessment of antioxidant activity of pure graphene oxide (GO) and composite V 2 O 5 /GO using DPPH radical and H 2 O 2 scavenging assays
Journal of Sol-Gel Science and Technology(2023)
摘要
In this research, the Co precipitation method was utilized to synthesize a nanocomposite of vanadium oxide (V 2 O 5 ) and graphene oxide (GO). Pure GO was synthesized by the modified hammers method. Using a 1:2 ratio of GO and V 2 O 5 and heating in the oven at 70 °C leading to the formation of V 2 O 5 /GO nanocomposite. By grafting of GO on V 2 O 5 surface, a high range of graphene oxidation in V 2 O 5 /GO allowed for better reduction with V 2 O 5 metal-oxide. The scanning electron microscope (SEM) images and X-ray diffraction (XRD) spectra provide evidence of the distinct phase of graphene oxide formation. The antioxidant activity of V 2 O 5 /GO nanocomposite was conducted in two vitro assays, focusing on neutralization of 2, 2-diphenyl-1-picrylhydrazyl (DPPH) and H 2 O 2 radicals. The uniqueness of the nanocomposite was evident from its concentration-dependent antioxidant activities. Interestingly, the V 2 O 5 /GO samples has showed 60% antioxidant performance in the H 2 O 2 assays compared to its constituent.
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关键词
Nanocomposite,Antioxidant,V2O5,Graphene,Co-precipitation method,Assays
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