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Small angle X-ray scattering of particle growth and structure in spray flame synthesis

Mira Simmler,Simon Buchheiser,Ricardo Tischendorf,Jalal Poostforooshan,Alfred P. Weber,Hans-Joachim Schmid,Hermann Nirschl

Applications in Energy and Combustion Science（2023）

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Abstract
•Small angle X-ray scattering and transmission electron microscopy for analysis.•Bimodality measured in primary particles of aggregates made by spray flame synthesis.•Small particle fraction identified in situ is formed via gas-to-particle pathway.•Large particle size dependent on burner, precursor composition and concentration.•Fractal dimension of mass point to diffusion-limited cluster aggregation.
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Key words
flame,particle growth,scattering,x-ray
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