Crystal Structure of Na 2 [OsCl 6 ]

O. V. Rudnitskaya,E. K. Kultyshkina,E. V. Dobrokhotova,T. A. Tereshina,A. S. Popova, Ya. V. Zubavichus,V. N. Khrustalev

Journal of Structural Chemistry（2019）

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摘要

Salt Na 2 [OsCl 6 ] is obtained by the interaction of H 2 [OsCl 6 ]·H 2 O with NaCl in boiling concentrated hydrochloric acid. According to the single crystal X-ray diffraction data, the substance crystallizes in the cubic system, space group Fm 3̄ m, a = 9.7461(11) Å, V= 925.8(3) Å 3 , Z = 4, R 1 = 0.029, wR 2 = 0.070. The compound is characterized by UV-vis and IR spectroscopy.

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关键词

osmium,osmium halide complexes,crystal structure,single crystal X-ray diffraction analysis

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