Microstructural evolution and interfacial properties of explosively welded Nb/steel composite plate during post-heat treatment

In this work, Nb/steel composite plates were fabricated by explosive welding technique. Then post-heat treatments were conducted for large temperature range of 723 K–1273 K. Microstructural evolution and interfacial properties in welded interface were revealed by SEM, EBSD, XRD, microhardness, nanohardness and shear strength examinations. The effects of annealed temperature on interfacial microstructures and properties of Nb/steel composites were systematically investigated. The results demonstrated that microstructures and microhardness of Nb-side almost presented no changes with annealed temperature; Carbon elements from steel-side diffused easily into Nb-side forming a thin Nb carbide layer in which content of NbC increased as increasing annealing temperature; At 1273 K, formation of Nb2C was also found in carbide layers. In the steel-side, during low temperature (723 K–923 K) annealing, the deformed pearlite near interface recrystallized to form ferrite of which grains grew up with increasing annealed temperature; During high temperature (1073 K–1273 K) annealing, a large number of voids appeared at 1073 K, and typical normalizing structure generated at 1173 K–1273 K. Meanwhile, it was also found that with increasing of annealed temperature, shear strength firstly increased to maximum value of 326 MPa at 923 K and then decreased to 267 MPa at 1273 K. Failure mechanism of shear tests exhibited mixed ductile-brittle fracture at low temperature annealing; Then it converted into brittle fracture at high temperature annealing. Microhardness near interface of steel side firstly decreased to the minimum value of 106HV at 923 K and then increased to value of 220HV at 1273 K.