Hollow fiber liquid-phase microextraction of multiclass pesticides in soil samples: A green analytical approach for challenging environmental monitoring analysis

Rafael Oliveira Martins, Gabriela Guimarães Souza,Lucas Santos Machado,Giovanna Lopes de Araújo,Rosineide Costa Simas, Bruno José Gonçalves da Silva, Virginia Damin,Andréa Rodrigues Chaves

Microchemical Journal(2023)

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Abstract
•Soil samples were evaluated by the two-phase HF-LPME method in “U” shape.•HF-LPME was successfully applied for multiclass pesticides extraction in soil.•The two-phase HF-LPME method could achieve recovery values ranging from 75 to 111 %.•LOD and LOQ values were obtained in the µg/L range.•An eco-friendly method was developed using µL of organic solvent.
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Key words
soil samples,multiclass pesticides,liquid-phase
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