A facile protocol for the preparation of 2-carboxylated thieno [2,3-b] indoles: a de novo access to alkaloid thienodolin

Giacomo Mari,Lucia De Crescentini,Gianfranco Favi,Stefania Santeusanio,Fabio Mantellini

Organic & Biomolecular Chemistry（2022）

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摘要

A metal-free strategy towards thieno [2,3-b] indoles from 1,2-diaza-1,3-dienes and indoline 2-thione is described. The mild reaction conditions required make this method amenable for a one-pot approach to thienodolin, a valuable natural alkaloid.

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