New Synthesis of Pine Sawfly Pheromones
Russian Journal of Organic Chemistry(2022)
Abstract
Based on the previously synthesized chiral intermediate, a new synthesis of pine sawfly pheromones bearing 3 stereocenters has been achieved. The key steps were Evans’ template induction, Wittig olefination, and conventional chemical operations. (2 S ,3 S ,7 S )-3,7-Dimethylpentadecan-2-yl acetate and propanoate were obtained in 9 steps with an overall yield of 34%.
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Key words
pine sawfly pheromones,stereocenters,(2S,3S,7S)-3,7-dimethylpentadecan-2-ol
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