Developing a Simple Scanning Probe System for Soft X-ray Spectroscopy with a Nano-focusing Mirror

E-JOURNAL OF SURFACE SCIENCE AND NANOTECHNOLOGY(2023)

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Abstract
We developed a compact system for the spectroscopic mapping of a microstructure with a nano-focused beam at a soft X-ray beamline of synchrotron radiation. The experimental setup com-prises a Wolter mirror and sample that are arranged with two mounting stages. The Wolter mirror is aligned with three degrees of freedom, and the sample with two degrees. The system gener-ates a beam with an 800-nm spot and maps out a chemical distri-bution of non-uniform material through near-edge X-ray fine structure spectroscopy. The design and actual system are suited to experiments conducted with a nano-focused X-ray beam at beam -lines of synchrotron radiation or an X-ray free-electron laser. Ad-ditionally, this technical note presents guidelines for actual experiments.
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Key words
X-ray spectroscopy,Nano-focusing mirror,Chemical map,Synchrotron radiation
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