n-BuLi-promoted nucleophilic addition of unactivated C(sp³)–H bonds to diazo compounds as N-terminal electrophiles: efficient synthesis of hydrazine derivatives

Lu Zhang,Ming Yang,Yue Gong,Jie Wang,Yu-Long Zhao

Organic Chemistry Frontiers（2023）

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摘要

A n-BuLi-promoted intermolecular nucleophilic addition of unactivated C(sp3)–H bonds to diazo compounds has been developed. This reaction provides a simple method for the synthesis of benzylhydrazines and alkylthio-substituted ethylhydrazines.

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关键词

hydrazine derivatives,nucleophilic addition,efficient synthesis,buli-promoted,n-terminal

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n-BuLi-promoted nucleophilic addition of unactivated C(sp3)–H bonds to diazo compounds as N-terminal electrophiles: efficient synthesis of hydrazine derivatives

n-BuLi-promoted nucleophilic addition of unactivated C(sp³)–H bonds to diazo compounds as N-terminal electrophiles: efficient synthesis of hydrazine derivatives