Photodimerization of (E)-3-(2,6-Difluorophenyl)-1-(4-methoxyphenyl)prop-2-en-1-one in the Crystalline Solid State
MOLBANK(2023)
Abstract
(E)-3-(2,6-difluorophenyl)-1-(4-methoxyphenyl)prop-2-en-1-one (1) was synthesized and characterized by H-1 and C-13 NMR, mass spectrometry, and single-crystal X-ray diffraction. Photolysis (lambda(irr) = 300 nm) of chalcone 1 in the crystalline solid state resulted in the stereospecific formation of the syn-head-to-head photodimer (beta-truxinic).
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Key words
(E)-3-(2,6-difluorophenyl)-1-(4-methoxyphenyl)prop-2-en-1-one,X-ray crystallography,photodimerization,beta-truxinic dimer
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