Characterization and isolation of an 18-crown-6 complex of potassium hydroxide prepared by milling: application to mechanochemical organic synthesis
NEW JOURNAL OF CHEMISTRY（2023）
Abstract
The enhanced mechanochemical reactivity of potassium hydroxide (KOH) in the presence of 18-crown-6 ether is supported by potassium complexation under milling and has been demonstrated in the Henry reaction and SNAr hydroxylation: in both cases, the desired product is formed within 10 minutes, but requires the presence of the crown ether.
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