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Photocatalyzed Synthesis of 3‐Substituted Phthalides: A Key Access to (±)‐Herbaric Acid

Lucas Fortier,Cyrille Gosset,Corentin Lefebvre,Sylvain Pellegrini,Lydie Pélinski,Till Bousquet

European Journal of Organic Chemistry（2023）

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Abstract
Abstract An efficient organophotocatalyzed protocol was developed for the preparation of 3‐substituted phthalides. The presented transformation was performed under particularly mild conditions within 6 h and was ultimately applied to a precursor of the herbaric acid.
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oxa-Michael cyclization,phthalides, photocatalysis,4-CzIPN,(±)-herbaric acid
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