8&#946;-Acetoxy-14&#945;-benzoyloxy-N-methyl-13&#946;,15&#945;-dihydroxy-1&#945;,6&#945;,16&#946;-trimethoxy-4&#946;-(methoxymethyl)aconitane: hypaconitine isolated from `fuzi'

Ling-Li Zheng, Yan Li,Tie-Ying Zi,Ming-Yong Yuan

Acta Crystallographica Section E（2010）

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Abstract

The title compound, C33H45NO10, has an aconitine carbon skeleton with four six-membered rings and two five-membered rings. The five-membered rings adopt envelope configurations and the six-membered N-containing heterocyclic ring displays a chair conformation. Two intramolecular O—H...O hydrogen bonds occur.

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8&amp;#946;-Acetoxy-14&amp;#945;-benzoyloxy-N-methyl-13&amp;#946;,15&amp;#945;-dihydroxy-1&amp;#945;,6&amp;#945;,16&amp;#946;-trimethoxy-4&amp;#946;-(methoxymethyl)aconitane: hypaconitine isolated from `fuzi'

8β-Acetoxy-14α-benzoyloxy-N-methyl-13β,15α-dihydroxy-1α,6α,16β-trimethoxy-4β-(methoxymethyl)aconitane: hypaconitine isolated from `fuzi'