Evaluation of the Fracture Toughness K_Ic for Selected Magnetron Sputtering Coatings by Using the Laugier Model

Nanoindentation is one of the methods that allows for determining the fracture properties of brittle materials. In this article, the authors present the possibility of the fracture toughness coefficient calculation of ceramic-based coatings doped by metal (W, Cr) by using the nanoindentation method with the Berkovich diamond indenter. The mechanical properties of selected coatings, such as hardness and Young's modulus, were investigated from nanohardness experiments. We analyzed the brittle fracture, which includes changes in hardness (H), Young's modulus (E), plasticity index H/E and resistance to plastic deformation H-3/E-2, enabled the concentration of tungsten and chromium. Due to the size of the indentation and the size of the initial cracks, it is necessary to use Scanning Electron Microscopy (SEM) to observe and measure the indentations made and the generated cracks. For evaluation of the fracture toughness in mode I, the Laugier model was chosen experimentally. The fracture toughness analysis showed that doping with concentrations of 10% W and 10% Cr causes an increase in the fracture toughness for K-Ic = 4.98 for TiBW (10%) and K-Ic = 6.23 for TiBCr (10%).