Understanding the agglomerate crystallisation of hexamine through X-ray microscopy and crystallographic modelling

Journal of Crystal Growth(2023)

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摘要
•Agglomerate growth with associated solvent inclusions observed in hexamine crystal powders.•3D X-Ray microscopy and crystallographic modelling study.•Agglomerates structure involves epitaxial orientation between constituent crystallites.•Inter-crystallite solution trapped by agglomeration forms inter-crystallite inclusions.•Growth mechanism: facet edge/corner instability coupled with lack of growth promoting dislocations.
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关键词
A1. Morphological stability,A1. Supersaturated solutions,A1. X-Ray computed tomography,A1. Computer simulation,A2. Growth from solutions
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