J-modulated F-19- and H-1-detected dual-optimized inverted (1)J(CC) 1,n-ADEQUATE: A universal ADEQUATE experiment

The recently reported F-19-detected dual-optimized inverted (1)J(CC) 1,n-ADEQUATE experiment and the previously reported H-1-detected version have been modified to incorporate J-modulation, making it feasible to acquire all 1,1- and 1,n-ADEQUATE correlations as well as (1)J(CC) and (n)J(CC) homonuclear scalar couplings in a single experiment. The experiments are demonstrated using N,N-dimethylamino-2,5,6-trifluoro-3,4-phthalonitrile and N,N-dimethylamino-3,4-phthalonitrile.