Development and competitive evaluation of methods for the reduction of (het)arylimines of cage-structured monoterpenoid ketones

R. V. Brunilin,A. A. Vernigora,O. V. Vostrikova, A. V. Davidenko,M. B. Nawrozkij, N. A. Salykin,I. A. Novakov

Russian Chemical Bulletin（2022）

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摘要

Various methods for the reduction of (het)arylimines of cage-structured monoterpenoid ketones, l -fenchone and d -camphor, were explored. The best results were achieved using the NaBH 4 -NiCl 2 • 6H 2 O system in 95% ethanol. The exception is halogenated aniline derivatives, in the case of which the reduction of the C-N bond is accompanied with the hydrogenolysis of the C-Hal bond.

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关键词

(het)arylimines of monoterpenoid ketones, reduction, actoprotectors, antiviral drugs, anti-aging agents for rubber compositions

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