Synthesis of the C19–C30 bis-THF fragment of iriomoteolide-13a via stepwise S_N2 cyclization and intramolecular syn-oxypalladation

Hui Zhao,Kai Gao,Haichen Ma,Tsz Chun Yip,Wei-Min Dai

Organic Chemistry Frontiers（2021）

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摘要

The bis-THF subunit of iriomoteolide-13a was stereoselectively constructed from the non-protected ene triol via syn-oxypalladation with excellent atom efficiency.

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Synthesis of the C19–C30 bis-THF fragment of iriomoteolide-13a via stepwise SN2 cyclization and intramolecular syn-oxypalladation

Synthesis of the C19–C30 bis-THF fragment of iriomoteolide-13a via stepwise S_N2 cyclization and intramolecular syn-oxypalladation