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Synthesis of Z-scheme g-C3N4/V2O5photocatalyst with high activity under visible light

Hung Thanh Tung Mai, Thi Hong Ngoc Doan, Ngoc Kim Tuyen Nguyen,Minh The Do,Van Hoang Cao,Thi Dieu Cam Nguyen

Ministry of Science and Technology, Vietnam(2021)

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Abstract
Direct Z-scheme g-C3N4/V2O5 photocatalysts were prepared through a sonication-assisted calcination method. The obtained samples were characterised by X-ray diffraction (XRD),Ultraviolet-visible diffuse reflectance spectroscopy (UV-Vis-DRS), Scanning electron microscope (SEM), andPhotoluminescence spectroscopy (PL). Oxidations of tetracycline hydrochloride (TC) were employed to evaluate the photocatalytic activities of the obtained g-C3N4/V2O5materials. Different weight ratios (5, 10, 15, and 20%) of g-C3N4/V2O5 loaded composites were prepared, in which a 15% (CV-15) loaded composite was found to show optimal catalytic performance for the reaction. The degradation conversation of TC has achieved approximately 79.67% in CV-15 after a 2-hour reaction. g-C3N4/V2O5 photocatalystwas more active than the individual g-C3N4 and V2O5 materials, which could be attributed to the efficient separation of photogenerated electron-hole pairs shown in the photocatalytic mechanism of TC degradation.
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Key words
g-c3n4/v2o5photocatalyst,synthesis,visible light,z-scheme
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