Development of a new approach for the synthesis of (+)-15-deoxy-Δ^12,14-prostaglandin J₂ methyl ester based on the [2+2]-cycloadduct of 5-trimethylsilylcyclopentadiene and dichloroketene

Airat M. Gimazetdinov,Aidar Z. Al’mukhametov, Mansur S. Miftakhov

New Journal of Chemistry（2022）

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摘要

This paper described a first example of the application of the “abnormal” lactone of 3-oxabicyclo[3.3.0]oct-6-en-2-one topology in targeted prostaglandin synthesis.

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methyl ester,synthesis,]-cycloadduct

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Development of a new approach for the synthesis of (+)-15-deoxy-Δ12,14-prostaglandin J2 methyl ester based on the [2+2]-cycloadduct of 5-trimethylsilylcyclopentadiene and dichloroketene

Development of a new approach for the synthesis of (+)-15-deoxy-Δ^12,14-prostaglandin J₂ methyl ester based on the [2+2]-cycloadduct of 5-trimethylsilylcyclopentadiene and dichloroketene