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温敏性环状聚合物的制备及表征

Nan Tingting,Gao Zhengguo,Lin Runxiong

Modern Plastics Processing and Applications（2022）

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Abstract
以溴化亚铜(CuBr)/三(2-二甲氨基乙基)胺(Me6TREN)为催化体系,2-氯丙酸炔丙酯(PCP)为引发剂,应用原子转移自由基聚合(ATRP)方法,引发保护炔基基团的甲基丙烯酸丙炔基酯与N-异丙基丙烯酰胺(NIP AM)共聚,得到末端带有炔基基团的线型聚合物,将线型聚合物叠氮化,使其两端分别带有炔基基团和叠氮基团,通过点击反应得到环状聚合物.当外界温度低于低临界溶解温度(LCST)时,环状聚合物溶液是澄清的;当外界温度高于LCST时,环状聚合物溶液是浑浊的,因此表现出良好的温敏性.
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