Phase Composition, Structure and Properties of the Spark Plasma Sintered Ceramics Obtained from the Al12Mg17-B-Si Powder Mixtures

NANOMATERIALS(2022)

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摘要
In this work, composite materials were obtained by spark plasma sintering of an Al12Mg17-B-Si powder mixture. The structure, phase composition, and mechanical properties of the obtained composites were studied. It was found that various compounds based on B-12 icosahedrons, such as AlB12, B4Si, and B6Si, are formed during spark plasma sintering. Based on the SEM images and results of XRD analysis of the obtained specimens, a probable scheme for the formation of the phase composition of composite materials during spark plasma sintering was proposed. An increase in the Al12Mg17-B powder content in the initial mixture from 30 to 70 wt% leads to an increase in hardness from 16.55 to 21.24 GPa and a decrease in the friction coefficient and wear rate from 0.56 to 0.32 and 13.60 to 5.60 10(-5) mm(-3)/(N/m), respectively.
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关键词
composite materials, B-12, silicon, spark plasma sintering, phase composition
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