Research on Microstructure Evolution of Deposited Metal of Low Nickel High Nitrogen Austenitic Stainless Steel

ADVANCES IN MATERIALS SCIENCE AND ENGINEERING(2021)

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摘要
In this paper, in situ observation of the cooling process of the deposited metal of low nickel high nitrogen austenitic stainless steel obtained by laser-arc hybrid surfacing welding with shielding gas containing only Ar and only N-2, respectively, is carried out using the ultra-high-temperature confocal laser scanning microscope (CLSM). An in-depth analysis of the microstructural changes is conducted with SEM, EDS, and EBSD. The results showed that the surface substructure is refined during crystallization with shielding gas Ar. However, grains are seriously coarsened in the delta phase area. Widmanstatten gamma and intragranular gamma are formed as a result of delta -> gamma phase transition through the shear-diffusion mechanism. In the cooling process with shielding gas N-2, the temperature range of each phase area narrowed obviously. Blocky gamma began to appear because of the delta -> gamma phase transition through the diffusion mechanism. Generally, Ar and N-2 have a strong effect only on the very shallow range from the surface. The area with a larger local misorientation with shielding gas Ar is at lath gamma on the surface. With shielding gas N-2, the large local misorientation area is the last contact position of gamma during the delta -> gamma phase transition on the surface and cross section.
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关键词
microstructure evolution,nickel,stainless steel
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