Simple and Inexpensive Method for the Detection of Carbon Monoxide Released from Thermal Cheletropic Decarbonylation Reactions
JOURNAL OF CHEMICAL EDUCATION(2021)
摘要
This work presents a simple protocol that demonstrates the use of an inexpensive household carbon monoxide detector as a useful tool to detect the release of carbon monoxide gas from thermal cheletropic decarbonylation reactions. The carbon monoxide detection method described has been employed in a short series of reactions used in a university teaching laboratory setting, and full procedures for these are outlined. In each case, the procedure to isolate and identify the decarbonylation products has also been provided.
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关键词
Upper-Division Undergraduate, Laboratory Instruction, Organic Chemistry, Hands-On Learning/Manipulatives, Problem Solving/Decision Making, Aromatic Compounds, Gases, Laboratory Equipment/Apparatus, Qualitative Analysis, X-ray Crystallography
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