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Synthesis of germanium sols via thermal decomposition of gaseous germane

Alexander A. Vinokurov,Konstantin O. Znamenkov,Sergey G. Dorofeev

Mendeleev Communications（2021）

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Abstract
A new approach to the synthesis of colloidal Ge nanoparticles in high-boiling solvent via thermal decomposition of germane is presented. Obtained products were analyzed by XRD, XRF, TEM, absorption spectrophotometry, Raman IR and PL spectroscopy. Ge nanoparticles have mean sizes about 4-5 nm, are apparently amorphous and nonspherical.
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Key words
germanium nanocrystals,germanium sols,germane,pyrolysis,amorphization,nanoparticles
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