Mono- and sym-pentahalogenated corannulenes: reaction optimization & purification by in process product analysis
Reaction Chemistry & Engineering（2022）
摘要
A robust, mild & inexpensive synthetic route to mono-halogenated corannulene and a robust method for purifying and analyzing sym-pentachlorocorannulene from the ICl halogenation of corannulene is reported.
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关键词
corannulenes,reaction optimization,purification
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