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[(CH3)2NH]3[H3PMo12O40]的合成、结构及表征

Xiao-jing LIU,Wei-dong TANG,Ying LIU,Zhi-meng LI,Cheng NIU,Fu-xiang WANG

Journal of Synthetic Crystals（2016）

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Abstract
通过水热合成法,成功合成了化合物[(CH3)2NH]3[H3PMo12O40],并通过单晶X射线衍射,IR,XRD,元素分析和电化学分析对该化合物进行表征.该化合物中,Keggin型磷钼酸之间通过氢键形成二维折叠层,这些层按照ABCD沿c轴方向堆积.二甲胺分子分布在层间,通过氢键连接相邻的来自不同层的两个Keggin型磷钼酸,将二维折叠层进一步拓展成三维超分子骨架.
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Key words
[(CH3)2NH]3[H3PMo12O40],hydrothermal synthesis,hydrogen bond,supramolecular
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