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Reaction of the Cationic Cluster [Os3(μ-H)(CO)10(μ-η1:η2-CCCMe2)]BF4 with Triphenylphosphine. Formation and Transformations of the σ-Acetylide Cluster [Os3(μ-H)(CO)10(PPh3)(σ-C⋮CCMe2PPh3)]BF4 and Two Isomeric Clusters [Os3(μ-H)(CO)9(PPh3)(μ-σ:η2-C⋮CCMe2PPh3)]BF4

Ol’ga A. Kizas,Vasily V. Krivykh,Evgenii V. Vorontsov,Oleg L. Tok,and Fedor M. Dolgushin,A.A. Koridze

Organometallics（2001）

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Abstract
The complex [Os3(μ-H)(CO)10(μ-η1:η2-CCCMe2)]BF4 (1) reacts with PPh3 at −78 °C to give isomeric phosphonium derivatives of the formula [Os3(μ-H)(CO)10(μ-σ:η2-C⋮CCMe2PPh3)]BF4 (2 and 3); the isomeri...
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Key words
cationic cluster,triphenylphosphine,isomeric clusters
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