One-Pot Synthesis of Cyclic Enecarbamates from Lactam Carbamates.

Jurong Yu,Vu Chi Truc,Peter Riebel,Elizabeth Hierl,Boguslaw Mudryk

ChemInform（2005）

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摘要

Abstract A general, practical and efficient one-pot synthesis of cyclic enecarbamates is described. The protocol proceeds via reduction of lactam carbamate with Super-Hydride ® , followed by in situ dehydration with trifluoroacetic anhydride (TFAA) and diisopropylethylamine (DIPEA).

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