Straightforward Functionalizationof 3,5-Dichloro-2-pyrazinones under Simultaneous Microwaveand Ultrasound Irradiation
Synthesis(2010)
摘要
Heck reactions and Suzuki-Miyaura cross-couplings with relatively poorly reactive 3,5-dichloro-2-pyrazinones were studied at the same temperature under conventional heating, dielectric heating (MW) and simultaneous MW/US irradiation. This comparative study showed a synergic effect of combined MW and US irradiation resulting in a much higher reaction yield, at the same time avoiding side reactions and partial degradation that is otherwise observed under conventional heating.
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关键词
simultaneous microwave
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