Flexible Sample Environment for the Investigation of Soft Matter at the European Spallation Source: Part II—The GISANS Setup
Applied Sciences(2021)
摘要
The FlexiProb project is a joint effort of three soft matter groups at the Universities of
Bielefeld, Darmstadt, and Munich with scientific support from the European Spallation Source (ESS),
the small-K advanced diffractometer (SKADI) beamline development group of the Julich Centre for
Neutron Science (JCNS), and the Heinz Maier-Leibnitz Zentrum (MLZ).Within this framework, a
flexible and quickly interchangeable sample carrier system for small-angle neutron scattering (SANS)
at the ESS was developed. In the present contribution, the development of a sample environment
for the investigation of soft matter thin films with grazing-incidence small-angle neutron scattering
(GISANS) is introduced. Therefore, components were assembled on an optical breadboard for the
measurement of thin film samples under controlled ambient conditions, with adjustable temperature
and humidity, as well as the optional in situ recording of the film thickness via spectral reflectance.
Samples were placed in a 3D-printed spherical humidity metal chamber, which enabled the accurate
control of experimental conditions via water-heated channels within its walls. A separately heated
gas flow stream supplied an adjustable flow of dry or saturated solvent vapor. First test experiments
proved the concept of the setup and respective component functionality.
更多查看译文
关键词
european spallation source,soft matter
AI 理解论文
溯源树
样例
生成溯源树,研究论文发展脉络
Chat Paper
正在生成论文摘要