Çözelti Plazma Sürecinde VOSO4•xH2O’nun Sulu Çözeltisi

In this work, the goal was to synthesize vanadium containing nanoparticles with solution plasma process (SPP) method.The solution plasma was produced by discharging with a bipolar DC power supply and the system was applied to 0.25 M aqueous solution of VOSO 4 •xH 2 O to prepare vanadium containing nanoparticles.The effects of different discharge times (0, 10, 20 and 30 minutes) and applied voltage (1500 V) during the synthesis were investigated.From all experiments same vanadium oxide compound(s)/mixture(s), named as "the product" and formulated as "V x O y ", were obtained.The product was tried to be characterized by using FTIR, TGA, DTA, XRD and FESEM-EDX analysis results.