Funktionalisierung von C 60 mit Nitriloxiden zu 4,5‐Dihydroisoxazolen und deren Strukturbestimmung
Chemische Berichte(1994)
摘要
Functionalization of C60 with Nitrile Oxides to 4,5-Dihydroisoxazoles and Their Structure Determination
Cycloadducts 3 of nitrile oxides 2 with C60 (1) are synthesized and isolated. The cycloadducts are characterized by 13C-NMR spectroscopy and high-resolution FAB mass spectrometry. X-ray structure determination of the 3-(9-anthryl)-4,5-dihydroisoxazole derivative 3a of C60 with CS2 included in the crystals is achieved at 173 K without disorder problems.
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关键词
nitriloxiden zu
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