非包覆型油井水泥自修复剂的制备与评价
Chinese Journal of Synthetic Chemistry（2021）
Abstract
采用反向悬浮聚合法,丙烯酸(AA)和丙烯酰胺(AM)为单体,过硫酸钾(KBS)作引发剂,N,N-亚甲基双丙烯酰胺(MBA)作交联剂,制备了一种非包覆遇水膨胀型自修复剂LF-1,其结构经SEM和IR表征.结果表明:LF-1分散均匀,表观形态呈多孔、粗糙褶皱状.将2％LF-1加入水泥浆中,水泥浆流动度为20.1 cm,失水52 mL,稠化时间217 min;用5000 mg/L的盐水养护造缝水泥石,12 h内即无渗透性;水泥石24 h抗压强度为16.1 MPa,抗折强度为4.92 MPa.
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