饲料中林可霉素检验方法研究

Livestock and Poultry Industry(2021)

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Abstract
实验应用气相层析质谱仪开发饲料中林可霉素残留检测方法.饲料经5%甲醇溶液萃取及卡瑞试剂沉淀蛋白质后,以hydrophilic-lipophilicbalance(HLB)材质固相萃取管纯化,再以N-methyl-N(trimethylsilyl)trifluoroacetamide(MST-FA)衍生化反应,使用内标准品检量线定量,所开发出的方法可成功地应用于饲料中林可霉素的残留检验.
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