Evaluation of a sensitive, reasonable, and fast detection method for 55Fe in steel
JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY(2021)
摘要
A pilot study to quantify 55Fe in steel from a reactor vessel of a nuclear power plant by accelerator mass spectrometry (AMS) without any chemical sample preparation was validated by liquid scintillation counting (LSC) and AMS after radiochemical separation. AMS reaches an uncertainty < 10% at the 1 kBq gFe−1 level within less than 10 min measuring time. The background was < 3 Bq gFe−1, presently limited by the short measurement time. The new instrumental AMS method for analysing 55Fe from neutron capture production is reasonable and fast compared to other analytical methods.
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关键词
Accelerator mass spectrometry,Nuclear decommissioning,Nuclear waste,55Fe,Radiochemical separation,Liquid scintillation counting
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