Catalytic Reductive Cleavage of Poly(phenylene sulfide) Using a Hydrosilane
SYNTHESIS-STUTTGART(2021)
Abstract
The solvent-insoluble poly(phenylene sulfide) main chain was reductively cleaved by using triethylsilane as a hydrogen source under palladium/IcHex catalytic conditions. After the reaction, benzene and bis(triethylsilyl) sulfide as a sulfide source were formed efficiently. This method could be operated on a gram scale.
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Key words
palladium,polymer,reduction,silane,sulfur
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