Progress On Optical Microspheres For Co2 Sensors

B. J. Demory,S. Harrison, C. Tolfa, L. T. Echeveria, P. K. Singh, V. V. Khitrov, K. G. Heinz, A. S-P Chang, T. Bond

LASER RESONATORS, MICRORESONATORS, AND BEAM CONTROL XXIII(2021)

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Abstract
Shrinking the volumetric footprint of gas sensors is desirable as it allows for nonintrusive, nonperturbing gas mixture analysis and access to tight enclosures. Micro-resonators are a perfect candidate for these sensors as their size parameter (similar to micron) is minimal, and the typical surface propagating whispering gallery modes can interact with an analyte without disrupting the environment. The large, quality factor (Q) of these resonant cavity modes enables long interaction lengths on the order of 100s of centimeters between the optical field and analyte. Thus, the presence of a gas different than the nominal environment will result in a shift of the resonant properties, including the resonant wavelength, amplitude, and quality factor, that can be detected in real-time. To illustrate this effect, we utilized a spherical micro resonator on the end of a piece of optical fiber, formed using standard ball lens fabrication, and excited the resonant modes using a tapered optical fiber connected to tunable Infrared laser. The resonator was fixed in contact with the tapered region of fiber, and the assembly was placed inside an in-house, optically coupled, vacuum-tight vessel for gas testing. We compared the spectral response of air, pure CO2, and pure N2 gas, observing spectral shifting and broadening of the cavity resonances. In addition, the effect of vessel temperature on resonance peak position due to the thermo-optic effect was investigated and quantified. Lastly, a feedback arm was added to the setup to reduce signal noise and automated data analysis was implemented to improve data clarity.
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Key words
Gas sensors, Optical resonators, CO2 detection, Microspheres
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